崔黎丽，中国人民解放军海军军医大学，教授， 军队院校“育才奖”银奖，总后优秀教师，上海市育才奖，学校特级教师、A级教师，最受学员喜爱的教师，上海市高校优秀青年教师等。

第一部分 绪论    

、物理化学实验的目的和要求

二、物理化学实验的安全知识

三、物理化学实验的设计思想和方法

四、误差理论和有效数字

五、实验数据的表示法

art One Introduction 

Objective   and  requirement

Physical chemistry laboratory safety

Rules and methods for designing of the physical chemistry experiment

Error theory and significant figures

Data reporting

第二部分 实验

art Two Experiments

实验一 燃烧热的测定

Experiment 1 Determination  of  Heats  of  Combustion

实验二 溶解热曲线的测定

Experiment 2 Determination of Heats of Solution Curve

实验三 凝固点降低法测定摩尔质量

Experiment 3 Determination of Molar Mass by Freezing  Point Depression

实验四 凝固点降低法测定氢化纳注射液的渗透压

Experiment 4 Determination of Osmotic Pressure of Sodium Chloride  Injection by Freezing Point Depression

实验五 静态法测定液体饱和蒸气压

Experiment 5 Saturated Vapor Pressure of Pure Liquids by Static Method

实验六 反应平衡常数及分配系数的测定

Experiment 6 Determination of Equilibrium Constant of Reaction and Partition Coefficient

实验七 二组分部分§溶双液系统目国的绘制

Experiment 7 Drawing of Phase Diagram for a Partially Miscible Binary Liquid System

实验八 完全§溶双液系统平衡目国的绘制

Experiment 8 Drawing of Phase Diagram for a Miscible Binary Liquid System

实验九 二组分简单低共熔系统目国的绘制

Experiment 9 Drawing of Phase Diagram for a Binary utectic System  76

实验十 三组分液－液系统目国的绘制    78

Experiment 10 Drawing of Phase Diagram for a Ternary Liquid System

实验十一 电解质水溶液电导的测定及应用

Experiment 11 Measurement and Application of lectrolyte Solution Conductance

实验十二 电动势法测溶液 pH 相反应热力学函数

xperiment 12 Determination of pH of Solutions and Thermodynamic Functions by lectromotive Force Measurements

实验十三 旋光法测定康糖转化反应的速率常数

Experiment 13 Determination of Rate Constant for the Conversion of Sucrose by Polarimetric Method

实验十四 乙酸乙醋皂化反应速率常数及活化能的测定  

Experiment 14 Determination of Rate Constant and Activation nergy for the Saponification of thyl Acetate by Conductometric Method

实验十五 腆化拥与过氧化氢反应的速率常数及活化能的测定  

Experiment 15 Determination of Rate Constant and Activation nergy for Reaction between Potassium Iodide and Hydrogen Peroxide

实验十六 丙酣漠化反应速率常数的测定  

Experiment 16 Determination of Rate Constant for the Bromination of Acetone

实验十七 最大气泡压力法测定液体表面张力  

Experiment 17 Determination of the Solution Surface Tension by Bubble Pressure  Method   

实验十八 固体在溶液中的眼附  

Experiment 18 Adsorption of Solids in Solution

实验十九 溶胶的制备及性质  

Experiment 19 Preparation and Properties of Sols

实验二十 黠度法测定大分子的平均目对分子质量  

Experiment 20 Determination of Average Relative Molar Mass of the Macromolecule by Viscosity Method

实验二十一 药物多晶型的差热分析（设计性实验) 

Experiment 21 Thermal Analysis of Polymorphism Pharmaceuticals（Designing xperiment)

实验二十二 药物稳定性及有效期测定（设计性实验) 

Experiment 22 Determination of Drug Stability and Shelf Life（Designing experiment)

实验二十三 载药纳米粒子的制备及表征（综合设计性实验) 

Experiment 23 Preparation and Characterization of Drug－loaded Nanoparticles（Comprehensive  Designing  xperiment) 

实验二十四 固体药物常规理化常数的测定（综合设计性实验) 

Sxperiment 24 Determination of Physical and Chemical Constants of Solid Drugs（Comprehensive   Designing xperiment)

实验二十五 表面活性剂临界胶束浓度的测定（综合设计性试验) 

Experiment 25 Determination of Critical Micelle Concentration for Surfactants（Comprehensive Designing xperiment)

实验二十六 乳状液的制备和性质（综合设计性实验) 

Experiment 26 Preparation and Properties of mulsion（Comprehensive Designing   xperiment)   

第三部分 实验测试题

一、单选题  

二、司口题 

 三、答案

art Three Experiment Test Questions

Section One Multiple  Choice  

Section Two Short Questions

Section Three Answers

第四部分 附录   

Part Four Appendices

一、 常用物理化学实验数据表（Common Data of xperimental Physical Chemistry)

二、 参考文献（References)